Technology Process of C62H70O8S4
There total 7 articles about C62H70O8S4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide; acetic acid / chloroform / 24 h / 20 °C
2.1: magnesium / diethyl ether / 3 h / Reflux
2.2: Inert atmosphere; Cooling; Reflux
3.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere; Reflux
3.2: 10 h / 0 - 20 °C / Inert atmosphere
4.1: thionyl chloride / 2 h / Reflux
5.1: dmap; triethylamine / dichloromethane / 4 h / Inert atmosphere
With
dmap; N-Bromosuccinimide; n-butyllithium; thionyl chloride; magnesium; acetic acid; triethylamine;
In
diethyl ether; hexane; dichloromethane; chloroform;
2.2: Kumada coupling reaction;
DOI:10.1039/c0jm01919d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 4 h / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / 1,4-dioxane / 40 °C / 2025.2 Torr
3: dmap; triethylamine / dichloromethane / 4 h / Inert atmosphere
With
dmap; palladium 10% on activated carbon; hydrogen; triethylamine;
In
1,4-dioxane; dichloromethane;
DOI:10.1039/c0jm01919d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / 2 h / Reflux
2: dmap; triethylamine / dichloromethane / 4 h / Inert atmosphere
With
dmap; thionyl chloride; triethylamine;
In
dichloromethane;
DOI:10.1039/c0jm01919d
