heptyl-m-tolyl ether

Base Information

Chemical Name:heptyl-m-tolyl ether
CAS No.:57792-37-7
Molecular Formula:C₁₄H₂₂O
Molecular Weight:206.328
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of heptyl-m-tolyl ether

Chemical Property:

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Technology Process of heptyl-m-tolyl ether

There total 2 articles about heptyl-m-tolyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 629-04-9
1-Bromoheptane

: 108-39-4
3-methyl-phenol

: 57792-37-7
heptyl-m-tolyl ether

Guidance literature:: With sodium amide; toluene;

Reference yield:

: 4282-40-0
1-Iodoheptane

: 108-39-4
3-methyl-phenol

: 57792-37-7
heptyl-m-tolyl ether

Guidance literature:: With potassium hydroxide;

Reference yield:

: 57792-37-7
heptyl-m-tolyl ether

: 1440060-31-0
C₂₃H₂₇F₂NO₂

Guidance literature:: Multi-step reaction with 6 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 5 - 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride / ethanol / 5 h / Reflux; Inert atmosphere

3: sodium tetrahydroborate; iodine / tetrahydrofuran / 7.5 h / 0 °C / Reflux; Inert atmosphere

4: triethylamine / tetrahydrofuran / 2 h / 5 - 20 °C / Inert atmosphere

5: thionyl chloride / toluene / 3 h / 80 °C / Inert atmosphere

6: sodium hydroxide / methanol / 1 h / 50 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; iodine; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; 1: |Friedel-Crafts Acylation;
DOI:10.1039/c3nj00032j