Technology Process of CH3C(CH2NHCOC5H3NCON(C2H5)2)2CH2NHCOC5H3NCONHC6H4CH2C6H4NHCOC5H3NCON(C2H5)2
There total 7 articles about CH3C(CH2NHCOC5H3NCON(C2H5)2)2CH2NHCOC5H3NCONHC6H4CH2C6H4NHCOC5H3NCON(C2H5)2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 0 - 20 °C
2: methanol; potassium hydroxide / dichloromethane / 2 h
3: tetrahydrofuran / 3 h / Reflux; Inert atmosphere
4: tetrahydrofuran / 18 h / Inert atmosphere; Reflux
With
methanol; triethylamine; potassium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja204474v
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 1 h / Inert atmosphere
2: triethylamine / dichloromethane / 0 - 20 °C
3: methanol; potassium hydroxide / dichloromethane / 2 h
4: tetrahydrofuran / 3 h / Reflux; Inert atmosphere
5: tetrahydrofuran / 18 h / Inert atmosphere; Reflux
With
methanol; thionyl chloride; triethylamine; N,N-dimethyl-formamide; potassium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja204474v
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 0 - 20 °C
2: methanol; potassium hydroxide / dichloromethane / 2 h
3: tetrahydrofuran / 3 h / Reflux; Inert atmosphere
4: tetrahydrofuran / 18 h / Inert atmosphere; Reflux
With
methanol; triethylamine; potassium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja204474v
