H₂-phencat

Base Information

• Chemical Name: H₂-phencat
• CAS No.: 1353662-41-5
• Molecular Formula: C₁₉H₁₃N₃O₃
• Molecular Weight: 331.331

Synonyms:

Chemical Property of H₂-phencat

Chemical Property:

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Technology Process of H₂-phencat

There total 1 articles about H₂-phencat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethoxy-N-(1,10-phenanthroline-5-yl)benzamide (947185-28-6) → H2-phencat (1353662-41-5)

Guidance literature:

2,3-dimethoxy-N-(1,10-phenanthroline-5-yl)benzamide; With boron tribromide; In dichloromethane; at -78 ℃; for 24h; Inert atmosphere;

With water; In dichloromethane; at -78 ℃; Inert atmosphere;

DOI:10.1039/c1dt11360g

Reference yield: 80.0%

potassium hexafluorophosphate (17084-13-8) + [iridium(III)(μ-chloro)(2-phenylpyridine)2]2 + H2-phencat (1353662-41-5) → (Ir(NC5H4C6H4)2(N2C12H7NHCOC6H3(OH)2))(1+)*PF6(1-)=(Ir(NC5H4C6H4)2(N2C12H7NHCOC6H3(OH)2))PF6

Guidance literature:

In methanol; other Radiation; (N2) Ir complex and ligand in MeOH was microwave irradiated for 20 min at 70°C, cooled to room temp., KPF6 was added, stirred for 30 min; solvent was removed in vacuo, residue was dissolved in CH2Cl2, filtered through Celite and concd., hexane was added, ppt. was filtered, washed with hexane and dried in vacuo; elem. anal.;

DOI:10.1039/c1dt11360g

Reference yield: 78.0%

potassium hexafluorophosphate (17084-13-8) + chloro(1-phenylpyrazole)iridium(III) dimer + H2-phencat (1353662-41-5) → (Ir(N2C3H3C6H4)2(N2C12H7NHCOC6H3(OH)2))(1+)*PF6(1-)=(Ir(N2C3H3C6H4)2(N2C12H7NHCOC6H3(OH)2))PF6

Guidance literature:

In methanol; other Radiation; (N2) Ir complex and ligand in MeOH was microwave irradiated for 20 min at 70°C, cooled to room temp., KPF6 was added, stirred for 30 min; solvent was removed in vacuo, residue was dissolved in CH2Cl2, filtered through Celite and concd., hexane was added, ppt. was filtered, washed with hexane and dried in vacuo; elem. anal.;

DOI:10.1039/c1dt11360g

upstream raw materials:

2,3-dimethoxy-N-(1,10-phenanthroline-5-yl)benzamide

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