N¹-(2-chloro-ethyl)-4-nitro-o-phenylenediamine

Base Information

• Chemical Name: N¹-(2-chloro-ethyl)-4-nitro-o-phenylenediamine
• CAS No.: 57944-32-8
• Molecular Formula: C₈H₁₀ClN₃O₂
• Molecular Weight: 215.639
• Mol file: 57944-32-8.mol

Synonyms:

Chemical Property of N¹-(2-chloro-ethyl)-4-nitro-o-phenylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N¹-(2-chloro-ethyl)-4-nitro-o-phenylenediamine

There total 3 articles about N¹-(2-chloro-ethyl)-4-nitro-o-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2'-hydroxy-ethyl)amino-2-amino-4-nitro-benzene (56932-44-6) → N1-(2-chloro-ethyl)-4-nitro-o-phenylenediamine (57944-32-8)

Guidance literature:

With thionyl chloride;

Reference yield:

N-(2,4-dinitrophenyl)aminoethanol (1945-92-2) → N1-(2-chloro-ethyl)-4-nitro-o-phenylenediamine (57944-32-8)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen sulfide; ethanolic ammonia

2: thionyl chloride

With thionyl chloride; hydrogen sulfide; ammonia;

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) → N1-(2-chloro-ethyl)-4-nitro-o-phenylenediamine (57944-32-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol

2: hydrogen sulfide; ethanolic ammonia

3: thionyl chloride

With thionyl chloride; ethanol; hydrogen sulfide; ammonia;

upstream raw materials:

1-(2'-hydroxy-ethyl)amino-2-amino-4-nitro-benzene

N-(2,4-dinitrophenyl)aminoethanol

1-chloro-2,4-dinitro-benzene

Downstream raw materials:

6-nitro-1,2,3,4-tetrahydroquinoxaline