[1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I)

Base Information

Chemical Name:[1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I)
CAS No.:86378-97-4
Molecular Formula:C₅H₅*C₂₇H₂₆P₂*Rh
Molecular Weight:580.451
Hs Code.:

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Chemical Property of [1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I)

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Technology Process of [1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I)

There total 1 articles about [1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: [dicarbonyldichlorodirhodium(I)]

: cyclopentadienylthallium(I)

: 86378-97-4
[1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I)

Guidance literature:: With dppp; In n-heptane; the soln. of intermediate was obtained from Rh complex and excess of Tlcomplex and refluxed with the ligand about 9 h under N2; the soln. was filtered, concd., pptd. by cooling to -30°C, elem.anal.;
DOI:10.1039/DT9830000433

Reference yield:

: 86378-97-4
[1,3-Bis(diphenylphosphino)propane]η-cyclopentadienylrhodium(I)

: 86379-01-3
[1,3-bis(diphenylphosphino)propane]η-cyclopentadienyl(methyl)rhodium(III) iodide

Guidance literature:: With MeI; In pentane; the excess of MeI was added dropwise to the stirred soln. of Rh complexunder N2; ppt. was washed with pentane, dried, elem. anal.;
DOI:10.1039/DT9830000433