Technology Process of C50H78INO8Si2
There total 2 articles about C50H78INO8Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere
2.2: 0.5 h / -78 °C / Inert atmosphere
3.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere
4.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
4.2: 12 h / 20 °C / Inert atmosphere
With
hydrogenchloride; zirconocene dichloride; sodium hydride; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; toluene; mineral oil;
DOI:10.1021/ol301103d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 0.5 h / -78 °C / Inert atmosphere
2.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere
3.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
3.2: 12 h / 20 °C / Inert atmosphere
With
hydrogenchloride; zirconocene dichloride; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; toluene;
DOI:10.1021/ol301103d
