cannabichromene

Base Information

• Chemical Name: cannabichromene
• CAS No.: 4993-99-1
• Molecular Formula: C₂₁H₃₀O₂
• Molecular Weight: 314.468
• Mol file: 4993-99-1.mol

Synonyms:

Chemical Property of cannabichromene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cannabichromene

There total 34 articles about cannabichromene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Olivetol (500-66-3) + (E/Z)-3,7-dimethyl-2,6-octadienal (5392-40-5,96680-15-8) → cannabichromene (20675-51-8,4993-99-1)

Guidance literature:

With ammonium chloride; In water; for 24h; Inert atmosphere; Reflux;

DOI:10.1021/acs.joc.0c02698

Reference yield: 65.0%

C15H26N(1+)*C2H3O2(1-) + Olivetol (500-66-3) → cannabichromene (20675-51-8,4993-99-1) + cannabicyclol (21366-63-2,67920-00-7)

Guidance literature:

In ethyl acetate; toluene; at 130 ℃; for 40h; Inert atmosphere;

DOI:10.1021/acs.jnatprod.1c00567

Reference yield: 55.0%

5-methoxy-2-methyl-2-(4-methyl-3-pentenyl)-7-pentyl-2H-chromene (57412-30-3) → cannabichromene (20675-51-8,4993-99-1)

Guidance literature:

With sodium hydride; ethanethiol; In N,N-dimethyl-formamide; for 1.5h; Heating;

DOI:10.1246/bcsj.68.305

upstream raw materials:

2-Methyl-2-(4-methyl-pent-3-enyl)-7-pentyl-6-phenylselanyl-2,6,7,8-tetrahydro-chromen-5-one

3,7-dimethyl-2,6-octadienal

Olivetol

5-methoxy-2-methyl-2-(4-methyl-3-pentenyl)-7-pentyl-2H-chromene

Downstream raw materials:

cannabicyclol

cannabicitran

cannabinol