2-amino-5-cyclopentyl-4-hydroxybenzonitrile

Base Information

Chemical Name:2-amino-5-cyclopentyl-4-hydroxybenzonitrile
CAS No.:1161025-12-2
Molecular Formula:C₁₂H₁₄N₂O
Molecular Weight:202.256
Hs Code.:

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Chemical Property of 2-amino-5-cyclopentyl-4-hydroxybenzonitrile

Chemical Property:

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Technology Process of 2-amino-5-cyclopentyl-4-hydroxybenzonitrile

There total 4 articles about 2-amino-5-cyclopentyl-4-hydroxybenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1161025-10-0
4-bromo-2-cyclopentyl-5-nitrophenyl methyl carbonate

: 1161025-12-2
2-amino-5-cyclopentyl-4-hydroxybenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 0.5 h / 130 °C / Microwave irradiation

2: hydrogen / palladium 10% on activated carbon / ethanol / 2 h

With hydrogen; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 55910-44-6
4-bromo-2-cyclopentylphenol

: 1161025-12-2
2-amino-5-cyclopentyl-4-hydroxybenzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dmap / dichloromethane / 2 h / 0 - 20 °C

2: sulfuric acid; nitric acid / 1 h / -10 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 0.5 h / 130 °C / Microwave irradiation

4: hydrogen / palladium 10% on activated carbon / ethanol / 2 h

With sulfuric acid; hydrogen; nitric acid; triethylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1518-84-9
2-cyclopentylphenol

: 1161025-12-2
2-amino-5-cyclopentyl-4-hydroxybenzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen bromide; acetic acid; dimethyl sulfoxide / water / 0.17 h

2: triethylamine / dmap / dichloromethane / 2 h / 0 - 20 °C

3: sulfuric acid; nitric acid / 1 h / -10 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 0.5 h / 130 °C / Microwave irradiation

5: hydrogen / palladium 10% on activated carbon / ethanol / 2 h

With sulfuric acid; hydrogen bromide; hydrogen; nitric acid; acetic acid; dimethyl sulfoxide; triethylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;