u-1,2-dibromo-1--2-phenylethane

Base Information

Chemical Name:u-1,2-dibromo-1--2-phenylethane
CAS No.:127233-02-7
Molecular Formula:C₂₆H₁₉Br₂Cl₃O₃Si
Molecular Weight:673.688
Hs Code.:

u-1,2-dibromo-1-<tris(p-chlorophenoxy)silyl>-2-phenylethane

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of u-1,2-dibromo-1--2-phenylethane

Chemical Property:

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Technology Process of u-1,2-dibromo-1--2-phenylethane

There total 8 articles about u-1,2-dibromo-1--2-phenylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127232-96-6
tris(p-chlorophenoxy)silane

: 127233-02-7,127233-05-0
l-1,2-dibromo-1--2-phenylethane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / (PPh₃)3RhCl / tetrahydrofuran; benzene / 48 h / 50 °C

2: bromine / diethyl ether / 0.5 h / -100 °C

With bromine; Wilkinson's catalyst; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo00298a043

Reference yield:

: 127232-96-6
tris(p-chlorophenoxy)silane

: 127233-02-7,127233-05-0
u-1,2-dibromo-1--2-phenylethane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / (PPh₃)3RhCl / tetrahydrofuran; benzene / 48 h / 50 °C

2: bromine / diethyl ether / 0.5 h / -100 °C

With bromine; Wilkinson's catalyst; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo00298a043

Reference yield:

: 106-48-9,82344-39-6
4-chloro-phenol

: 127233-02-7,127233-05-0
l-1,2-dibromo-1--2-phenylethane

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 4 h / 65 °C

2: 70 percent / (PPh₃)3RhCl / tetrahydrofuran; benzene / 48 h / 50 °C

3: bromine / diethyl ether / 0.5 h / -100 °C

With bromine; Wilkinson's catalyst; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo00298a043