5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene

Base Information

• Chemical Name: 5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene
• CAS No.: 77333-74-5
• Molecular Formula: C₂₅H₂₂
• Molecular Weight: 322.45

Synonyms:

Chemical Property of 5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene

Chemical Property:

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Technology Process of 5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene

There total 2 articles about 5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

3-methyl-1,2-diphenyl-3-(o-allylphenyl)cyclopropene (77333-71-2) → 1,1a,6,6a-tetrahydro-1a-methyl-exo-1,6a-diphenyl-endo-6-ethenylcyclopropindene (70913-16-5) + 5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene (77333-74-5) + 4-Methyl-2,3-diphenyl-1-vinyl-1,2-dihydro-naphthalene (77333-73-4)

Guidance literature:

Irradiation;

DOI:10.1021/ja00397a056

Reference yield:

3-methyl-1,2-diphenyl-3-(o-allylphenyl)cyclopropene (77333-71-2) → trans-1,2-dihydro-4-methyl-2,3-diphenyl-1-ethenylnaphthalene (89121-23-3) + 1,1a,6,6a-tetrahydro-1a-methyl-exo-1,6a-diphenyl-endo-6-ethenylcyclopropindene (70913-16-5) + 5,5a,6,11,11a,12-hexahydro-5-methyl-5a-phenylcyclopropa-naphthacene (77333-74-5)

Guidance literature:

With thio-xanthene-9-one; In benzene; for 1.25h; Irradiation;

DOI:10.1021/jo00182a008

upstream raw materials:

3-methyl-1,2-diphenyl-3-(o-allylphenyl)cyclopropene

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