4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin

Base Information

Chemical Name:4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin
CAS No.:88489-45-6
Molecular Formula:C₃₁H₃₅O₆P
Molecular Weight:534.589
Hs Code.:

4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<d,g><1,3,2>dioxaphosphocin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin

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Technology Process of 4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin

There total 2 articles about 4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 88489-47-8
2,2'-methylenebis(6-tert-butyl-4-methoxycarbonylphenol)

: 644-97-3
Dichlorophenylphosphine

: 88489-45-6
4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin

Guidance literature:: With triethylamine; In toluene; Ambient temperature; overnight;

Reference yield:

: 39778-63-7
3-(1,1-dimethylethyl)-4-hydroxybenzoic acid methyl ester

: 88489-45-6
4,8-di-t-butyl-2,10-bis(carbomethoxy)-6-phenyl-12H-dibenzo<1,3,2>dioxaphosphocin

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / potassium t-butoxide / 1,2,3,4-tetrahydro-naphthalene / 3 h / 170 °C

2: 73 percent / triethylamine / toluene / Ambient temperature; overnight

With potassium tert-butylate; triethylamine; In tetralin; toluene;