C₃₄H₃₇NO₈S

Base Information

• Chemical Name: C₃₄H₃₇NO₈S
• CAS No.: 231609-80-6
• Molecular Formula: C₃₄H₃₇NO₈S
• Molecular Weight: 619.736
• Mol file: 231609-80-6.mol

Synonyms:

Chemical Property of C₃₄H₃₇NO₈S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₇NO₈S

There total 8 articles about C₃₄H₃₇NO₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1-(3-bromoprop-1-en-1-yl)naphthalene (98978-42-8) → C34H37NO8S (231609-80-6)

Guidance literature:

Multi-step reaction with 7 steps

1: 85 percent / aq. NH₄Cl, Zn / tetrahydrofuran

2: 80 percent / aq. LiOH / tetrahydrofuran

4: aq. NaHCO₃ / CH₂Cl₂

5: OsO₄, NaIO₄ / tetrahydrofuran; H₂O

6: LiAl(OtBu)3H / CH₂Cl₂ / -40 - -5 °C

7: pyridine, DMAP / CH₂Cl₂

With pyridine; dmap; lithium hydroxide; sodium periodate; osmium(VIII) oxide; sodium hydrogencarbonate; ammonium chloride; lithium tri-t-butoxyaluminum hydride; zinc; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/S0960-894X(99)00218-8

Reference yield:

(2S,3S)-2-Benzyloxyamino-3-naphthalen-1-yl-pent-4-enoic acid → C34H37NO8S (231609-80-6)

Guidance literature:

Multi-step reaction with 5 steps

2: aq. NaHCO₃ / CH₂Cl₂

3: OsO₄, NaIO₄ / tetrahydrofuran; H₂O

4: LiAl(OtBu)3H / CH₂Cl₂ / -40 - -5 °C

5: pyridine, DMAP / CH₂Cl₂

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; sodium hydrogencarbonate; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/S0960-894X(99)00218-8

Reference yield:

(2S,3S)-2-Benzyloxyamino-3-naphthalen-1-yl-pent-4-enoic acid tert-butyl ester → C34H37NO8S (231609-80-6)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. NaHCO₃ / CH₂Cl₂

2: OsO₄, NaIO₄ / tetrahydrofuran; H₂O

3: LiAl(OtBu)3H / CH₂Cl₂ / -40 - -5 °C

4: pyridine, DMAP / CH₂Cl₂

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; sodium hydrogencarbonate; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/S0960-894X(99)00218-8

upstream raw materials:

methanesulfonyl chloride

(E)-1-(3-bromoprop-1-en-1-yl)naphthalene

C₃₄H₃₅NO₅

(2S,3S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-naphthalen-1-yl-pent-4-en-1-one