ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside
CAS No.:134662-22-9
Molecular Formula:C₉₈H₁₀₈O₁₉S
Molecular Weight:1621.99
Hs Code.:

ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

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Chemical Property of ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

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Technology Process of ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

There total 1 articles about ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-24-7
acetic anhydride

: 134662-21-8
ethyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-1-thio-α-L-rhamnopyranoside

: 134662-22-9
ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: In pyridine;
DOI:10.1016/0008-6215(91)80096-6

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 134662-22-9
ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

: C₉₆H₁₀₄O₂₀

: 134662-23-0,134732-29-9
3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

Guidance literature:: With silver silicate; bromine; Yield given. Multistep reaction; 1) CH₂Cl₂, 10 min; 2) toluene, CH₂Cl₂, 2 h;
DOI:10.1016/0008-6215(91)80096-6