5-deuterio-5,7-diphenyldibenzazepine

Base Information

Chemical Name:5-deuterio-5,7-diphenyldibenzazepine
CAS No.:106569-16-8
Molecular Formula:C₂₆H₁₉N
Molecular Weight:346.436
Hs Code.:

5-deuterio-5,7-diphenyldibenz<c,e>azepine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-deuterio-5,7-diphenyldibenzazepine

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Technology Process of 5-deuterio-5,7-diphenyldibenzazepine

There total 3 articles about 5-deuterio-5,7-diphenyldibenzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [2'-(Amino-phenyl-methyl)-biphenyl-2-yl]-phenyl-methanone

: 106569-16-8
5-deuterio-5,7-diphenyldibenzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. 4-toluenesulfonic acid / acetone / 10 h / Heating

2: 1.) LDA, 2.) D₂O / 1.) THF, -78 deg C, 4 h, 2.) -40 deg C

With water-d2; toluene-4-sulfonic acid; lithium diisopropyl amide; In acetone;
DOI:10.1021/jo00380a010

Reference yield:

: 106568-98-3,106568-99-4
<2'-(2-phenyl-1,3-dioxolan-2-yl)<1,1'-biphenyl>-2-yl>phenylmethanone oxime

: 106569-16-8
5-deuterio-5,7-diphenyldibenzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: Zn, concd. NH₃, ammonium aceatate / Heating

2: aq. 4-toluenesulfonic acid / acetone / 10 h / Heating

3: 1.) LDA, 2.) D₂O / 1.) THF, -78 deg C, 4 h, 2.) -40 deg C

With ammonium hydroxide; ammonium acetate; water-d2; toluene-4-sulfonic acid; zinc; lithium diisopropyl amide; In acetone;
DOI:10.1021/jo00380a010

Reference yield:

: 106569-03-3
5,7-diphenyl-5H-dibenzazepine

: 106569-16-8
5-deuterio-5,7-diphenyldibenzazepine

Guidance literature:: With water-d2; lithium diisopropyl amide; Multistep reaction; 1.) THF, -78 deg C, 4 h, 2.) -40 deg C;
DOI:10.1021/jo00380a010