tin(II)(benzoin semicarbazone)

Base Information

Chemical Name:tin(II)(benzoin semicarbazone)
CAS No.:103948-23-8
Molecular Formula:C₁₅H₁₃N₃O₂Sn
Molecular Weight:385.997
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tin(II)(benzoin semicarbazone)

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Technology Process of tin(II)(benzoin semicarbazone)

There total 1 articles about tin(II)(benzoin semicarbazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 27538-28-9
2-hydroxy-2-phenylacetophenone semicarbazone

: tin(ll) chloride

: 103948-23-8
tin(II)(benzoin semicarbazone)

Guidance literature:: With triethylamine; In tetrahydrofuran; byproducts: NH(C2H5)3Cl; addn. of a calcd. amt. of the semicarbazone and NEt3 to anhyd. SnCl2 in dry THF under N2; stirring for about 1 h;; NHEt3Cl was filtered off; removal of solvent from the filtrate; the residue was washed repeatedly with dry cyclohexane and dried at 40+/-5°C (bath temp.) under vac.; elem. anal.;;
DOI:10.1016/S0277-5387(00)84430-7