Ac-Leu-Asn--Ile-Val-OMe

Base Information

Chemical Name:Ac-Leu-Asn--Ile-Val-OMe
CAS No.:127231-49-6
Molecular Formula:C₃₆H₆₅N₇O₉
Molecular Weight:739.954
Hs Code.:

Synonyms:

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Chemical Property of Ac-Leu-Asn--Ile-Val-OMe

Chemical Property:

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Technology Process of Ac-Leu-Asn--Ile-Val-OMe

There total 12 articles about Ac-Leu-Asn--Ile-Val-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54793-58-7
L-isoleucyl-L-valine methyl ester

: 127231-49-6,127306-20-1,137328-41-7
Ac-Leu-Asn--Ile-Val-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) N-methylmorpholine, 2.) isobutyl chloroformate

2: H₂ / Pd/C

3: NaI, NaHCO₃ / dimethylformamide

4: NaBH₄ / methanol

With 4-methyl-morpholine; sodium tetrahydroborate; hydrogen; sodium hydrogencarbonate; sodium iodide; isobutyl chloroformate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00167a003

Reference yield:

: 33911-17-0
N-tert-butoxycarbonyl (S)-isoleucine (S)-valine methyl ester

: 127231-49-6,127306-20-1,137328-41-7
Ac-Leu-Asn--Ile-Val-OMe

Guidance literature:: Multi-step reaction with 5 steps

1: 4 N HCl / dioxane

2: 1.) N-methylmorpholine, 2.) isobutyl chloroformate

3: H₂ / Pd/C

4: NaI, NaHCO₃ / dimethylformamide

5: NaBH₄ / methanol

With 4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; hydrogen; sodium hydrogencarbonate; sodium iodide; isobutyl chloroformate; palladium on activated charcoal; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00167a003

Reference yield:

: 127231-57-6
Z-Pro-Ile-Val-OMe

: 127231-49-6,127306-20-1,137328-41-7
Ac-Leu-Asn--Ile-Val-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C

2: NaI, NaHCO₃ / dimethylformamide

3: NaBH₄ / methanol

With sodium tetrahydroborate; hydrogen; sodium hydrogencarbonate; sodium iodide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00167a003