Technology Process of C19H28O4
There total 7 articles about C19H28O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 20 - 80 ℃;
DOI:10.1002/ejoc.201402234
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; cesium fluoride / N,N-dimethyl-formamide / 1.5 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 80 °C
With
lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; cesium fluoride;
In
tetrahydrofuran; N,N-dimethyl-formamide;
1: |Stille Cross Coupling;
DOI:10.1002/ejoc.201402234
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / dimethyl sulfoxide / 2 h / 0 - 20 °C
1.2: 5 h / 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; cesium fluoride / N,N-dimethyl-formamide / 1.5 h / 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 80 °C
With
lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; sodium hydride; cesium fluoride;
In
tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
2.1: |Stille Cross Coupling;
DOI:10.1002/ejoc.201402234
