Methanesulfonato{[4-(N,N-dimethylamino)phenyl]di-t-butylphosphino}(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [Amphos Palladacycle Gen. 3]

Base Information

• Chemical Name: Methanesulfonato{[4-(N,N-dimethylamino)phenyl]di-t-butylphosphino}(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [Amphos Palladacycle Gen. 3]
• CAS No.: 1820817-64-8
• Molecular Formula: C₂₉H₄₁N₂O₃PPdS
• Molecular Weight: 635.116

Synonyms:

Chemical Property of Methanesulfonato{[4-(N,N-dimethylamino)phenyl]di-t-butylphosphino}(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [Amphos Palladacycle Gen. 3]

Chemical Property:

• Melting Point: 192-201 °C (decomposition)
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

Methanesulfonato{[4-(N,N-dimethylamino)phenyl]di-t-butylphosphino}(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [Amphos Palladacycle Gen. 3] ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: APhos Pd G3 is a Buchwald precatalyst that can be used in cross-coupling reactions.

Technology Process of Methanesulfonato{[4-(N,N-dimethylamino)phenyl]di-t-butylphosphino}(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [Amphos Palladacycle Gen. 3]

There total 1 articles about Methanesulfonato{[4-(N,N-dimethylamino)phenyl]di-t-butylphosphino}(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [Amphos Palladacycle Gen. 3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine (932710-63-9) + μ-OMs dimer → [4-(di-tert-butylphosphino)-N,N-dimethylaniline-2-(2’-aminobiphenyl)]palladium(II) methanesulfonate (1820817-64-8)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.joc.1c01252

upstream raw materials:

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine

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