Δ^9,11-hexahydrocannabinol

Base Information

• Chemical Name: Δ^9,11-hexahydrocannabinol
• CAS No.: 16964-52-6
• Molecular Formula: C₂₁H₃₀O₂
• Molecular Weight: 314.468
• Mol file: 16964-52-6.mol

Synonyms:

Chemical Property of Δ^9,11-hexahydrocannabinol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Δ^9,11-hexahydrocannabinol

There total 2 articles about Δ^9,11-hexahydrocannabinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-α-chlorohexahydrocannabinol (17990-25-9,121694-19-7,121694-20-0) → Δ9,11-hexahydrocannabinol (16849-44-8,16964-52-6,27179-28-8,32794-91-5)

Guidance literature:

With potassium 2-methylbutan-2-olate; In benzene; Yield given; 1) 0 deg C, 30 min, 2) 70 deg C, 3 h;

DOI:10.1002/jhet.5570250324

Reference yield:

(+)-trans-Δ8-tetrahydrocannabinol (6087-61-2) → Δ9,11-hexahydrocannabinol (16849-44-8,16964-52-6,27179-28-8,32794-91-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / HCl (g), ZnCl₂ / CH₂Cl₂ / 2 h / -60 °C

2: potassium t-amylate / benzene / 1) 0 deg C, 30 min, 2) 70 deg C, 3 h

With hydrogenchloride; potassium 2-methylbutan-2-olate; zinc(II) chloride; In dichloromethane; benzene;

DOI:10.1002/jhet.5570250324

upstream raw materials:

9-α-chlorohexahydrocannabinol

(+)-trans-Δ⁸-tetrahydrocannabinol