(3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane

Base Information

Chemical Name:(3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane
CAS No.:128803-08-7
Molecular Formula:C₃₄H₄₄F₆O₆
Molecular Weight:662.71
Hs Code.:

Synonyms:

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Chemical Property of (3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane

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Technology Process of (3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane

There total 27 articles about (3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 110971-16-9
(+)-(3S)-tetradecane-1,3-diol

: 128803-08-7
(3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane

Guidance literature:: With pyridine; for 12h; Ambient temperature;

Reference yield:

: 26186-02-7
tridec-1-yne

: 128803-08-7,128898-82-8
(S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-[2-((S)-3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-ethyl]-dodecyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 1) DIBAH / 1) hexane 2) toluene, ether

2: 1) m-chloroperoxybenzoic acid, NaHCO₃ 2) pyridine / 1) CH₂Cl₂, 0-4 deg C, 20h 2) THF, 1h, r.t.

3: 99 percent / n-Bu₄NF / tetrahydrofuran / Ambient temperature

4: sodium dihydrobis(2-methoxyethoxy)aluminate (Red-Al) / tetrahydrofuran; toluene / Ambient temperature

5: cyclohexene, 1N aq. HCl / 10percent Pd/C / methanol / Heating

6: NaIO₄ / methanol; H₂O / Ambient temperature

7: NaBH₄ / ethanol / Ambient temperature

8: pyridine

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; cyclohexene; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water; toluene;

Reference yield:

: 26186-02-7
tridec-1-yne

: 128803-08-7
(3S)-1,3-Bis<(S)-α-methoxy-α-(trifluoromethyl)phenylacetoxy>tetradecane

Guidance literature:: Multi-step reaction with 8 steps

1: 1) DIBAH / 1) hexane 2) toluene, ether

2: 1) m-chloroperoxybenzoic acid, NaHCO₃ 2) pyridine / 1) CH₂Cl₂, 0-4 deg C, 20h 2) THF, 1h, r.t.

3: 99 percent / n-Bu₄NF / tetrahydrofuran / 0.33 h / Ambient temperature

4: 19.6 mg / sodium dihydrobis(2-methoxyethoxy)aluminate (Red-Al) / tetrahydrofuran; toluene / 6 h / Ambient temperature

5: 13.6 mg / cyclohexene, 1N aq. HCl / 10percent Pd/C / methanol / 2 h / Heating

6: 8.7 mg / NaIO₄ / methanol; H₂O / 1 h / Ambient temperature

7: 1.2 mg / NaBH₄ / ethanol / 1 h / Ambient temperature

8: 97 percent / pyridine / 12 h / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; cyclohexene; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water; toluene;