4-Chloro-N-(2-dibenzofuranylmethylene)benzenamine

Base Information

• Chemical Name: 4-Chloro-N-(2-dibenzofuranylmethylene)benzenamine
• CAS No.: 51818-92-9
• Molecular Formula: C₁₉H₁₂ClNO
• Molecular Weight: 305.763
• DSSTox Substance ID: DTXSID101234677

Synonyms:DTXSID101234677;4-Chloro-N-(2-dibenzofuranylmethylene)benzenamine;51818-92-9

Chemical Property of 4-Chloro-N-(2-dibenzofuranylmethylene)benzenamine

Chemical Property:

• XLogP3: 6.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 305.0607417
• Heavy Atom Count: 22
• Complexity: 404

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=C(O2)C=CC(=C3)C=NC4=CC=C(C=C4)Cl

Technology Process of 4-Chloro-N-(2-dibenzofuranylmethylene)benzenamine

There total 1 articles about 4-Chloro-N-(2-dibenzofuranylmethylene)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibenzofuran (132-64-9,214827-48-2) → 4-chloro-N-dibenzofuran-2-ylmethylene-aniline (51818-92-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tin(IV) chloride / dichloromethane / 0.67 h / 20 °C

2: tin(II) chloride dihdyrate; sodium sulfate / acetonitrile / 0.25 h / 20 °C

With tin(II) chloride dihdyrate; tin(IV) chloride; sodium sulfate; In dichloromethane; acetonitrile;

DOI:10.1016/j.ejmech.2011.06.014

Reference yield:

2-(4-methylphenyl)-5-phenyl-1,3,4-oxadiazole (1874-47-1) + 4-chloro-N-dibenzofuran-2-ylmethylene-aniline (51818-92-9) → 2-[4-(trans-2-dibenzofuran-2-yl-vinyl)-phenyl]-5-phenyl-[1,3,4]oxadiazole (52822-95-4)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide;

DOI:10.1002/hlca.19740570402

Reference yield:

6-Phenyl-2-(p-tolyl)benzoxazol (16156-02-8) + 4-chloro-N-dibenzofuran-2-ylmethylene-aniline (51818-92-9) → 2-[4-(trans-2-dibenzofuran-2-yl-vinyl)-phenyl]-6-phenyl-benzooxazole (52822-94-3)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide;

DOI:10.1002/hlca.19740570402

upstream raw materials:

dibenzofuran

Downstream raw materials:

2-[4-(trans-2-dibenzofuran-2-yl-vinyl)-phenyl]-5-phenyl-[1,3,4]oxadiazole

2-[4-(trans-2-dibenzofuran-2-yl-vinyl)-phenyl]-6-phenyl-benzooxazole

2-[4-(trans-2-dibenzofuran-2-yl-vinyl)-phenyl]-5-phenyl-benzooxazole

2-[4-(trans-2-dibenzofuran-2-yl-vinyl)-phenyl]-5-(4-methoxy-phenyl)-[1,3,4]oxadiazole

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