C₃₅H₄₂N₄O₇S₂

Base Information

Chemical Name:C₃₅H₄₂N₄O₇S₂
CAS No.:1403834-77-4
Molecular Formula:C₃₅H₄₂N₄O₇S₂
Molecular Weight:694.873
Hs Code.:

C<sub>35</sub>H<sub>42</sub>N<sub>4</sub>O<sub>7</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₃₅H₄₂N₄O₇S₂

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Technology Process of C₃₅H₄₂N₄O₇S₂

There total 2 articles about C₃₅H₄₂N₄O₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 151-10-0
1,3-Dimethoxybenzene

: 1403834-77-4
C₃₅H₄₂N₄O₇S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane / 0.33 h / 0 - 20 °C / Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: N-chloro-succinimide / dichloromethane / 0.5 h / -30 °C / Inert atmosphere; Irradiation

2.2: 0.5 h / -30 °C / Inert atmosphere; Irradiation

3.1: diisopropyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 1.08 h / 20 °C / Inert atmosphere

3.2: rink amide resin / Inert atmosphere

With N-chloro-succinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol3025499 DOI:10.1021/ol3025499

Reference yield:

: 26163-11-1
2,6-dimethoxybenzenethiol

: 1403834-77-4
C₃₅H₄₂N₄O₇S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chloro-succinimide / dichloromethane / 0.5 h / -30 °C / Inert atmosphere; Irradiation

1.2: 0.5 h / -30 °C / Inert atmosphere; Irradiation

2.1: diisopropyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 1.08 h / 20 °C / Inert atmosphere

2.2: rink amide resin / Inert atmosphere

With N-chloro-succinimide; ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol3025499 DOI:10.1021/ol3025499

Reference yield:

: 1403834-77-4
C₃₅H₄₂N₄O₇S₂

: C₂₀H₃₂N₄O₅S₂

Guidance literature:: C₃₅H₄₂N₄O₇S₂; In dichloromethane; N,N-dimethyl-formamide; Inert atmosphere;

With piperidine; In dichloromethane; N,N-dimethyl-formamide; Further stages; Inert atmosphere;
DOI:10.1021/ol3025499 DOI:10.1021/ol3025499