Technology Process of C30H45O6S(1-)*Li(1+)
There total 9 articles about C30H45O6S(1-)*Li(1+) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
sodium 2-(2-(2-(2-(4-(5-dodecylthiophen-2-yl)phenoxy)ethoxy)ethoxy)ethoxy)acetate;
With
hydrogenchloride; water;
In
diethyl ether;
With
lithium hydroxide;
In
diethyl ether;
at 20 ℃;
for 12h;
DOI:10.1002/cjoc.201280021
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron tribromide / dichloromethane / 24 h / -78 - 20 °C
2.1: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 6 h / Reflux
3.1: sodium hydride / tetrahydrofuran / 1.5 h / Reflux
3.2: 15 h / Reflux
4.1: hydrogenchloride; water / diethyl ether
4.2: 12 h / 20 °C
With
hydrogenchloride; tetrabutylammomium bromide; water; boron tribromide; sodium hydride; potassium carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/cjoc.201280021
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 6 h / Reflux
2.1: sodium hydride / tetrahydrofuran / 1.5 h / Reflux
2.2: 15 h / Reflux
3.1: hydrogenchloride; water / diethyl ether
3.2: 12 h / 20 °C
With
hydrogenchloride; tetrabutylammomium bromide; water; sodium hydride; potassium carbonate;
In
tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1002/cjoc.201280021
