Technology Process of C36H26O6
There total 6 articles about C36H26O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 150 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / chloroform / 72 h / 20 °C / Cooling with ice; Darkness
3: potassium hydroxide / methanol / 0.5 h / Reflux
With
potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; potassium hydroxide;
In
methanol; chloroform; N,N-dimethyl-formamide;
2: Baeyer-Villiger oxidation;
DOI:10.1021/ma201599p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / chloroform / 72 h / 20 °C / Cooling with ice; Darkness
2: potassium hydroxide / methanol / 0.5 h / Reflux
With
3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; potassium hydroxide;
In
methanol; chloroform;
1: Baeyer-Villiger oxidation;
DOI:10.1021/ma201599p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen bromide; acetic acid / 16 h / 160 °C
2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 150 °C / Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / chloroform / 72 h / 20 °C / Cooling with ice; Darkness
4: potassium hydroxide / methanol / 0.5 h / Reflux
With
hydrogen bromide; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; potassium hydroxide;
In
methanol; chloroform; N,N-dimethyl-formamide;
3: Baeyer-Villiger oxidation;
DOI:10.1021/ma201599p
