C₂₇H₃₇N₅O₄

Base Information

Chemical Name:C₂₇H₃₇N₅O₄
CAS No.:1408288-12-9
Molecular Formula:C₂₇H₃₇N₅O₄
Molecular Weight:495.622
Hs Code.:

C<sub>27</sub>H<sub>37</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₇N₅O₄

Chemical Property:

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Technology Process of C₂₇H₃₇N₅O₄

There total 5 articles about C₂₇H₃₇N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₅₃N₅O₈

: 1408288-12-9
C₂₇H₃₇N₅O₄

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja309172t

Reference yield:

: C₄₁H₅₄N₄O₁₁

: 1408288-12-9
C₂₇H₃₇N₅O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: manganese(III) triacetate dihydrate; acetic acid / 60 °C / Inert atmosphere

2.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere

3.1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere

4.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere

4.2: 18 h / 50 °C / Inert atmosphere

5.1: water; triphenylphosphine / tetrahydrofuran / 18 h / 60 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

With calcium borohydride bis(tetrahydrofuran); diphenyl phosphoryl azide; water; manganese(III) triacetate dihydrate; acetic acid; triphenylphosphine; trifluoroacetic acid; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja309172t

Reference yield:

: 1408288-11-8
C₄₀H₅₃N₇O₉

: 1408288-12-9
C₂₇H₃₇N₅O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere

1.2: 18 h / 50 °C / Inert atmosphere

2.1: water; triphenylphosphine / tetrahydrofuran / 18 h / 60 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

With calcium borohydride bis(tetrahydrofuran); water; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja309172t