sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate

Base Information

• Chemical Name: sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate
• CAS No.: 80103-60-2
• Molecular Formula: C₆H₂N₃O₇*C₁₆H₃₂N₂O₅*Na
• Molecular Weight: 583.528
• Mol file: 80103-60-2.mol

Synonyms:

Chemical Property of sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate

There total 2 articles about sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

sodium picrate (3324-58-1) + 4,7,13,16,21-Pentaoxa-1,10-diaza-bicyclo[8.8.5]tricosane (31364-42-8) → sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate (80103-60-2)

Guidance literature:

at 25 ℃;

DOI:10.1021/ja00298a041

Reference yield:

C50H48O6*C6H2N3O7(1-)*Na(1+) (82484-55-7) + 4,7,13,16,21-Pentaoxa-1,10-diaza-bicyclo[8.8.5]tricosane (31364-42-8) → sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate (80103-60-2)

Guidance literature:

With triethylamine; In chloroform-d1; water-d2; at 25 ℃; Equilibrium constant; Thermodynamic data;

DOI:10.1021/ja00298a041

Reference yield:

11,12,24,25-tetrahydro-28,34-dimethoxy-3,6,16,19,31,37-hexamethyl-1,21<1',3'>:8,14<1'',3''>-dibenzeno-10H,23H-tetrabenzo<1,5,10,14>tetraoxacyclooctadecin (95782-47-1,95782-45-9,73229-33-1) + sodium 4,7,13,16,21-pentaoxa-1,10-diazabicyclo<8.8.5>tricosane picrate (80103-60-2) → C50H48O6*C6H2N3O7(1-)*Na(1+) (82484-55-7)

Guidance literature:

With triethylamine; In chloroform-d1; water-d2; at 25 ℃; Equilibrium constant; Thermodynamic data;

DOI:10.1021/ja00298a041

upstream raw materials:

sodium picrate

4,7,13,16,21-Pentaoxa-1,10-diaza-bicyclo[8.8.5]tricosane

C₅₀H₄₈O₆*C₆H₂N₃O₇^(1-)*Na⁽¹⁺⁾

Downstream raw materials:

C₅₀H₄₈O₆*C₆H₂N₃O₇^(1-)*Na⁽¹⁺⁾