pentamethylene-5 pentadiene-3,4 amide

Base Information

Chemical Name:pentamethylene-5 pentadiene-3,4 amide
CAS No.:86517-42-2
Molecular Formula:C₁₂H₁₉NO
Molecular Weight:193.289
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentamethylene-5 pentadiene-3,4 amide

Chemical Property:

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Technology Process of pentamethylene-5 pentadiene-3,4 amide

There total 3 articles about pentamethylene-5 pentadiene-3,4 amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 71800-23-2
pentamethylene-5 pentadiene-3,4 nitrile

: 86517-42-2
pentamethylene-5 pentadiene-3,4 amide

Guidance literature:: With dihydrogen peroxide; sodium carbonate; In methanol; for 1h; Heating;

Reference yield:

: 71800-27-6
pentamethylene-5 pentadiene-3,4 al-oxime

: 86517-42-2
pentamethylene-5 pentadiene-3,4 amide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / PCl₅ / diethyl ether / 4 h

2: 60 percent / 50percent H₂O₂, 6N aq. Na₂CO₃ / methanol / 1 h / Heating

With phosphorus pentachloride; dihydrogen peroxide; sodium carbonate; In methanol; diethyl ether;

Reference yield:

: 6038-03-5
4-cyclohexylidene-2,2-dimethyl-3-butenal

: 86517-42-2
pentamethylene-5 pentadiene-3,4 amide

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH*HCl, Na₂CO₃ / methanol / 10 h / Ambient temperature

2: 50 percent / PCl₅ / diethyl ether / 4 h

3: 60 percent / 50percent H₂O₂, 6N aq. Na₂CO₃ / methanol / 1 h / Heating

With phosphorus pentachloride; hydroxylamine hydrochloride; dihydrogen peroxide; sodium carbonate; In methanol; diethyl ether;