Technology Process of C16H11Br4N5OS
There total 3 articles about C16H11Br4N5OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / AlCl3 / 2 h / Heating
2: 63 percent / NH2OH*HCl, pyridine / 3 h / Heating
3: 85 percent / N2H4*H2O / butan-1-ol / 6 h / Heating
4: 1.) NH4OH, 2.) 50percent N2H4*H2O, ClCH2COONa
With
pyridine; ammonium hydroxide; aluminium trichloride; hydroxylamine hydrochloride; sodium monochloroacetic acid; hydrazine hydrate;
In
butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / AlCl3 / 2 h / Heating
2: 63 percent / NH2OH*HCl, pyridine / 3 h / Heating
3: 85 percent / N2H4*H2O / butan-1-ol / 6 h / Heating
4: 1.) NH4OH, 2.) 50percent N2H4*H2O, ClCH2COONa
With
pyridine; ammonium hydroxide; aluminium trichloride; hydroxylamine hydrochloride; sodium monochloroacetic acid; hydrazine hydrate;
In
butan-1-ol;
- Guidance literature:
-
With
ammonium hydroxide; sodium monochloroacetic acid; hydrazine hydrate;
Yield given. Multistep reaction;