[5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine

Base Information

• Chemical Name: [5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine
• CAS No.: 145696-03-3
• Molecular Formula: C₂₃H₁₈ClN₉O₂S₂
• Molecular Weight: 552.04

Synonyms:

Chemical Property of [5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine

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Technology Process of [5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine

There total 1 articles about [5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

5-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-3-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2-thioxo-thiazolidin-4-one (134961-36-7) → [5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine (145696-03-3)

Guidance literature:

With hydrazine hydrate; In ethanol; for 4h; Heating;

Reference yield: 60.0%

[5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine (145696-03-3) → [5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-benzenesulfonyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine (145696-10-2)

Guidance literature:

With dihydrogen peroxide; acetic acid; for 72h; Ambient temperature;

upstream raw materials:

5-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-3-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-2-thioxo-thiazolidin-4-one

Downstream raw materials:

[5-[2-(4-Chloro-phenyl)-1-hydrazono-ethyl]-4-[6-(4-nitro-benzenesulfonyl)-benzothiazol-2-yl]-2,4-dihydro-[1,2,4]triazol-(3Z)-ylidene]-hydrazine

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