6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide

Base Information

• Chemical Name: 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide
• CAS No.: 79233-06-0
• Molecular Formula: C₂₄H₃₀O₃S
• Molecular Weight: 398.566
• Mol file: 79233-06-0.mol

Synonyms:

Chemical Property of 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide

There total 6 articles about 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-3,7-dimethylocta-2,6-diene (5389-87-7) → 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide (79233-06-0,79233-50-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Na / 1.) Et₂O, 3 h, 2.) reflux, overnight

2: 27.8 g / anhyd. K₂CO₃ / acetone / 6 h / Heating

3: 1.) anhyd. Na₂CO₃, 2.) DMF / 1.) CH₂Cl₂, -50 deg C -> room temperature; reflux, overnight, 2.) 100 deg C, 90 min

4: 7.3 g / sodium metaperiodate / ethanol; H₂O / 1.) 0 deg C, 4 h, 2.) room temperature, overnight

With sodium periodate; sodium; sodium carbonate; potassium carbonate; N,N-dimethyl-formamide; In ethanol; water; acetone;

DOI:10.1039/P19810001849

Reference yield:

(E)-2-(3,7-dimethylocta-2,6-dien-1-yl)-4-methoxyphenol (79233-10-6) → 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide (79233-06-0,79233-50-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 27.8 g / anhyd. K₂CO₃ / acetone / 6 h / Heating

2: 1.) anhyd. Na₂CO₃, 2.) DMF / 1.) CH₂Cl₂, -50 deg C -> room temperature; reflux, overnight, 2.) 100 deg C, 90 min

3: 7.3 g / sodium metaperiodate / ethanol; H₂O / 1.) 0 deg C, 4 h, 2.) room temperature, overnight

With sodium periodate; sodium carbonate; potassium carbonate; N,N-dimethyl-formamide; In ethanol; water; acetone;

DOI:10.1039/P19810001849

Reference yield:

4-methoxy-phenol (150-76-5) → 6-(2,5-dimethoxyphenyl)-1-isopropenyl-4-methylhex-4-enyl phenyl sulphoxide (79233-06-0,79233-50-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Na / 1.) Et₂O, 3 h, 2.) reflux, overnight

2: 27.8 g / anhyd. K₂CO₃ / acetone / 6 h / Heating

3: 1.) anhyd. Na₂CO₃, 2.) DMF / 1.) CH₂Cl₂, -50 deg C -> room temperature; reflux, overnight, 2.) 100 deg C, 90 min

4: 7.3 g / sodium metaperiodate / ethanol; H₂O / 1.) 0 deg C, 4 h, 2.) room temperature, overnight

With sodium periodate; sodium; sodium carbonate; potassium carbonate; N,N-dimethyl-formamide; In ethanol; water; acetone;

DOI:10.1039/P19810001849

upstream raw materials:

1,4-dimethoxy-2-(3,7-dimethyl-6-phenylthio-octa-3,7-dienyl)benzene

(E)-2-(3,7-dimethylocta-2,6-dien-1-yl)-4-methoxyphenol

4-methoxy-phenol

2-(3,7-Dimethyl-2,6-octadien-1-yl) 1,4-dimethoxybenzene

Downstream raw materials:

8-(2,5-dimethoxyphenyl)-2,6-dimethylocta-2,6-dienol

8-(2,5-dimethoxyphenyl)-2,6-dimethylocta-2,6-dienol

2,6-dimethyl-8-(2,5-dimethoxyphenyl)octa-2,6-dienal

di-O-methylalliodorin