3,5-dinitro-benzoic acid undec-2-enyl ester

Base Information

• Chemical Name: 3,5-dinitro-benzoic acid undec-2-enyl ester
• CAS No.: 93948-06-2
• Molecular Formula: C₁₈H₂₄N₂O₆
• Molecular Weight: 364.398
• Mol file: 93948-06-2.mol

Synonyms:

Chemical Property of 3,5-dinitro-benzoic acid undec-2-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3,5-dinitro-benzoic acid undec-2-enyl ester

There total 2 articles about 3,5-dinitro-benzoic acid undec-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

octylmagnesium bromide (17049-49-9) → 3,5-dinitro-benzoic acid undec-2-enyl ester (93948-06-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erwaermen des erhaltenen Alkohols mit PBr₃ in Gegenwart von Pyridin, Kochen des entstandenen Bromids mit Eisessig und Natriumacetat und Verseifen des Reaktionsprodukts mit siedender waessrig-methylalkoholischer NaOH

With diethyl ether;

DOI:10.1021/ja01172a601

Reference yield:

trans-2-undecen-1-ol (75039-83-7,75039-84-8,37617-03-1) → 3,5-dinitro-benzoic acid undec-2-enyl ester (93948-06-2)

Guidance literature:

DOI:10.1021/ja01172a601

upstream raw materials:

trans-2-undecen-1-ol

octylmagnesium bromide