p-methoxybenzyltartronic acid monoamide

Base Information

• Chemical Name: p-methoxybenzyltartronic acid monoamide
• CAS No.: 105955-68-8
• Molecular Formula: C₁₁H₁₃NO₅
• Molecular Weight: 239.228

Synonyms:

Chemical Property of p-methoxybenzyltartronic acid monoamide

Chemical Property:

Purity/Quality:

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Technology Process of p-methoxybenzyltartronic acid monoamide

There total 1 articles about p-methoxybenzyltartronic acid monoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(p-methoxyphenyl)-2,3-diketobutyramide hydrate (133373-30-5) → p-methoxybenzyltartronic acid monoamide (105955-68-8)

Guidance literature:

With hydrogenchloride; sodium hydroxide; In water; 1) 0 deg C, 30 min; 2) 0 deg C;

DOI:10.1002/hlca.19850680807

Reference yield:

p-methoxybenzyltartronic acid monoamide (105955-68-8) → 2-hydroxy-3-(4-methoxyphenyl)propanoic acid (33173-34-1,28030-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.7 g / 0.08 h / 150 °C

2: acid hydrolysis

DOI:10.1002/hlca.19850680807

Reference yield:

p-methoxybenzyltartronic acid monoamide (105955-68-8) → 3-(p-methoxyphenyl)lactamide

Guidance literature:

at 150 ℃; for 0.0833333h;

DOI:10.1002/hlca.19850680807

upstream raw materials:

4-(p-methoxyphenyl)-2,3-diketobutyramide hydrate

Downstream raw materials:

2-hydroxy-3-(4-methoxyphenyl)propanoic acid

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