(pentamethylcyclopentadienyl)germanium chloride

Base Information

Chemical Name:(pentamethylcyclopentadienyl)germanium chloride
CAS No.:85085-98-9
Molecular Formula:C₁₀H₁₅*Cl*Ge
Molecular Weight:243.272
Hs Code.:

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Chemical Property of (pentamethylcyclopentadienyl)germanium chloride

Chemical Property:

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Technology Process of (pentamethylcyclopentadienyl)germanium chloride

There total 1 articles about (pentamethylcyclopentadienyl)germanium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 310407-26-2
(C₅(CH₃)5GeC₅(CH₃)2H₂)2C₆H₄

: tin(ll) chloride

: 85085-98-9
(pentamethylcyclopentadienyl)germanium(II)-chloride

: 460740-94-7
C₅(CH₃)5Ge⁽¹⁺⁾*SnCl₃^(1-)=C₅(CH₃)5GeSnCl₃

: 111690-90-5
p-bis(3,4-dimethylcyclopentadienyl)benzene

Guidance literature:: In tetrahydrofuran; (N2); addn. of a soln. of SnCl2 in THF to a soln. of germanium complex in THF at -78°C, stirring for 1 h at -40°C; concn., addn. of hexane, addn. of THf to ppt., concn., detected by NMR;
DOI:10.1016/S0022-328X(02)01221-4

Reference yield: 59.0%

: 85085-98-9
(pentamethylcyclopentadienyl)germanium chloride

: 35383-91-6
2,4,6-tri-tert-butylphenyllithium

: 136630-27-8
(pentamethylcyclopentadienyl)(2,4,6-tri-tert-butylphenyl)germylene

Guidance literature:: In tetrahydrofuran; hexane; toluene; byproducts: LiCl; (Ar), Ge-complex in toluene and freshly prepared Li-compound in THF/hexane(10:1) added at -80°C whithin 2 h, allowed to warm up to room temp. very slowly; solvent evapd. in vac., residue extd. with hexane, concn., cooling to -25°C; elem. anal.;
DOI:10.1021/om00057a012

Reference yield: 40.0%

: trans-bisdinitrogenbis(1,2-diphenylphosphinoethane)molybdenum⁽⁰⁾

: 85085-98-9
pentamethylcyclopentadienylgermanium chloride

: 108-88-3,15644-74-3,16713-13-6
toluene

: bis(pentamethylcyclopentadienyl)germanium

: trans-[MoCl₂(1,2-bis(diphenylphosphino)ethane)2]

: trans-[Mo(1,2-bis(diphenylphosphino)ethane)2ClGe(η1-C5(CH3)5)]-toluene

Guidance literature:: In toluene; byproducts: N2; the suspn. in toluene was refluxed for 20 min; warm soln. was filtered, concd., cooled to -28°C for 1 h, ppt. was washed with cold toluene, dried in vac., recrystd. from toluene, driedunder vac. at ambient temp.; elem. anal.;
DOI:10.1021/om010785x