methyl 2-(S)--3-iodopropionate

Base Information

Chemical Name:methyl 2-(S)--3-iodopropionate
CAS No.:121080-47-5
Molecular Formula:C₁₇H₂₀INO₄
Molecular Weight:429.255
Hs Code.:

methyl 2-(S)-<N-benzyloxycarbonyl-N-(2-(1R,S)-cyclopenten-1-yl)amino>-3-iodopropionate

Synonyms:

Suppliers and Price of methyl 2-(S)--3-iodopropionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2-(S)--3-iodopropionate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2-(S)--3-iodopropionate

There total 4 articles about methyl 2-(S)--3-iodopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.3%

: 121080-46-4
N-benzyloxycarbonyl-N-(2-(1R,S)-cyclopenten-1-yl)-L-serine methyl ester

: 121080-47-5
methyl 2-(S)--3-iodopropionate

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In benzene; for 5h; Ambient temperature;
DOI:10.3987/COM-88-S111

Reference yield:

: 36291-48-2
3-bromocyclopentene

: 121080-47-5
methyl 2-(S)--3-iodopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / K₂CO₃ / acetonitrile / 2 h / Ambient temperature

2: 90 percent / NaHCO₃ / H₂O / 1.33 h

3: 45.3 percent / triphenylphosphine, imidazole, iodine / benzene / 5 h / Ambient temperature

With 1H-imidazole; iodine; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; In water; acetonitrile; benzene;
DOI:10.3987/COM-88-S111

Reference yield:

: 121080-45-3
N-(2-(1R,S)-cyclopenten-1-yl)-L-serine methyl ester

: 121080-47-5
methyl 2-(S)--3-iodopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaHCO₃ / H₂O / 1.33 h

2: 45.3 percent / triphenylphosphine, imidazole, iodine / benzene / 5 h / Ambient temperature

With 1H-imidazole; iodine; sodium hydrogencarbonate; triphenylphosphine; In water; benzene;
DOI:10.3987/COM-88-S111