Technology Process of C15H20O4Se
There total 11 articles about C15H20O4Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 1.) MeLi / 2.) -78 deg C
2: tetrahydrofuran / -78 °C
3: PPTS / methanol
4: 85 percent / NMO / OsO4 / tetrahydrofuran; H2O / 0 °C
5: 90 percent / NaHCO3 / methanol
6: DIBAL-H / CH2Cl2 / -78 °C
7: BF3*Et2O / -78 °C
8: O3 / -78 °C
With
N-methyl-2-indolinone; boron trifluoride diethyl etherate; methyllithium; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium hydrogencarbonate; ozone;
osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)96757-1
- Guidance literature:
-
Multi-step reaction with 10 steps
2: tetrahydrofuran / -78 °C
3: 1.) MeLi / 2.) -78 deg C
4: tetrahydrofuran / -78 °C
5: PPTS / methanol
6: 85 percent / NMO / OsO4 / tetrahydrofuran; H2O / 0 °C
7: 90 percent / NaHCO3 / methanol
8: DIBAL-H / CH2Cl2 / -78 °C
9: BF3*Et2O / -78 °C
10: O3 / -78 °C
With
N-methyl-2-indolinone; boron trifluoride diethyl etherate; methyllithium; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium hydrogencarbonate; ozone;
osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)96757-1
- Guidance literature:
-
Multi-step reaction with 9 steps
1: tetrahydrofuran / -78 °C
2: 1.) MeLi / 2.) -78 deg C
3: tetrahydrofuran / -78 °C
4: PPTS / methanol
5: 85 percent / NMO / OsO4 / tetrahydrofuran; H2O / 0 °C
6: 90 percent / NaHCO3 / methanol
7: DIBAL-H / CH2Cl2 / -78 °C
8: BF3*Et2O / -78 °C
9: O3 / -78 °C
With
N-methyl-2-indolinone; boron trifluoride diethyl etherate; methyllithium; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium hydrogencarbonate; ozone;
osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)96757-1