1,5-dibis(1,3-thiazolidine-2-thione)

Base Information

• Chemical Name: 1,5-dibis(1,3-thiazolidine-2-thione)
• CAS No.: 171416-83-4
• Molecular Formula: C₁₇H₁₉N₃O₄S₅
• Molecular Weight: 489.686

Synonyms:

Chemical Property of 1,5-dibis(1,3-thiazolidine-2-thione)

Chemical Property:

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Technology Process of 1,5-dibis(1,3-thiazolidine-2-thione)

There total 1 articles about 1,5-dibis(1,3-thiazolidine-2-thione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

thallium salt of Δ2-1,3-thiazoline-2-thiol (63987-96-2) + N-Tosyliminodiacetic acid dichloroanhydride (42031-77-6) → 1,5-dibis(1,3-thiazolidine-2-thione) (171416-83-4)

Guidance literature:

In tetrahydrofuran; for 48h;

DOI:10.1055/s-1995-4043

Reference yield: 84.0%

1,5-dibis(1,3-thiazolidine-2-thione) (171416-83-4) + 1,7-di(2'-aminoethyl)-4,10-di(p-toluenesulfonyl)-1,4,7,10-tetraazacyclododecane (171416-85-6) → 5,9-dioxo-7,16,21-tri(p-toluenesulfonyl)-1,4,7,10,13,16,21-heptaazabicyclo<11.5.5>tricosane

Guidance literature:

In dichloromethane; for 1h;

DOI:10.1055/s-1995-4043

Reference yield: 44.0%

1,5-dibis(1,3-thiazolidine-2-thione) (171416-83-4) + 1,7-di(3'-propylamine)-4,10-di(p-toluenesulfonyl)-1,4,7,10-tetraazacyclododecane → 6,10-dioxo-8,18,23-tri(p-toluenesulfonyl)-1,5,8,11,15,18,23-heptaazabicyclo<13.5.5>pentaicosane

Guidance literature:

In dichloromethane;

DOI:10.1055/s-1995-4043

upstream raw materials:

thallium salt of Δ²-1,3-thiazoline-2-thiol

N-Tosyliminodiacetic acid dichloroanhydride

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