C₂₈H₂₄

Base Information

Chemical Name:C₂₈H₂₄
CAS No.:135295-98-6
Molecular Formula:C₂₈H₂₄
Molecular Weight:360.499
Hs Code.:

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Suppliers and Price of C₂₈H₂₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₄

Chemical Property:

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Technology Process of C₂₈H₂₄

There total 5 articles about C₂₈H₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135295-97-5
C₂₈H₂₆

: 135295-98-6
C₂₈H₂₄

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; Heating;
DOI:10.1039/P19910001221

Reference yield:

: 23697-29-2
9,10-Benzo-bicyclo[3.3.2]dec-9-en-3,7-dion

: 135295-98-6
C₂₈H₂₄

Guidance literature:: Multi-step reaction with 5 steps

1: 1) butyllithium / 1) THF, -70 deg C to 0 deg C, 2) THF, a) -70 deg C, 2 h, b) to room temp.

2: 100 percent / tetrahydrofuran / 24 h

3: 83 percent / Na/Hg, disodium hydrogen orthophosphate / tetrahydrofuran; methanol / 1) -70 deg C to -20 deg C, 2) -20 deg C, 3 h, 3) -20 deg C to room temp., 4) room temp, 8 h

4: toluene-p-sulphonic acid monohydrate / 52 h / 120 °C

5: N-bromosuccinimide (NBS) / CCl₄ / Heating

With disodium hydrogenphosphate; sodium amalgam; N-Bromosuccinimide; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; tetrachloromethane;
DOI:10.1039/P19910001221

Reference yield:

: 135295-89-5,136031-17-9,136031-18-0
13-Phenethylidene-tricyclo[6.3.3.0^2,7]tetradeca-2,4,6-trien-10-one

: 135295-98-6
C₂₈H₂₄

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-p-sulphonic acid monohydrate / 52 h / 120 °C

2: N-bromosuccinimide (NBS) / CCl₄ / Heating

With N-Bromosuccinimide; toluene-4-sulfonic acid; In tetrachloromethane;
DOI:10.1039/P19910001221