1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene

Base Information

Chemical Name:1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene
CAS No.:474687-12-2
Molecular Formula:C₄₅H₈₀GeSi₆
Molecular Weight:862.233
Hs Code.:

Synonyms:

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Chemical Property of 1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene

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Technology Process of 1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene

There total 1 articles about 1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 412356-78-6
dibromo(2,6-diisopropylphenyl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)germane

: 583-53-9
2,3-dibromobenzene

: 474687-12-2
1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene

Guidance literature:: With lithium naphthalenide; In tetrahydrofuran; reduction of dibromogermane with 5 equivs. of lithium naphthalenide in THF at -78°C, addn. of 1 equiv. of 1,2-dibromobenzene; chromy., recrystn. from hexane/ethanol; elem. anal.;
DOI:10.1021/om020545x

Reference yield: 63.0%

: 10544-50-0
sulfur

: 474687-12-2
1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene

: 847335-79-9
2-(2,6-diisopropylphenyl)-2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2H-benzo[c][1,2]thiagermete

Guidance literature:: In benzene-d6; High Pressure; (Ar); heating a soln. of germanium compd. and sulfur in C6D6 in a sealedNMR tube at 135°C for 120 h; sepn. by HPLC (toluene), preparative thin layer chromy. (hexane); elem. anal.;
DOI:10.1021/om049216q

Reference yield: 56.0%

: 7782-49-2
selenium

: 474687-12-2
1-(2,6-diisopropylphenyl)-1-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1-germacyclopropabenzene

: 847335-80-2
2-(2,6-diisopropylphenyl)-2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2H-benzo[c][1,2]selenagermete

Guidance literature:: In benzene-d6; High Pressure; (Ar); heating a suspn. of germanium compd. and Se in C6D6 in a sealed NMR tube at 135°C for 216 h; sepn. by preparative thin layer chromy. (hexane); elem. anal.;
DOI:10.1021/om049216q