DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

Base Information

Chemical Name:DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat
CAS No.:112297-36-6
Molecular Formula:C₁₉H₂₂BrNO₈S
Molecular Weight:504.356
Hs Code.:

DL-(1α,2β,3α,4α,5β,6α)-5-<Acetyl(4-methylphenylsulfonyl)amino>-3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

Synonyms:

Suppliers and Price of DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

There total 2 articles about DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 108-24-7
acetic anhydride

: 112297-34-4
DL-(1α,2β,3α,4α,5β,6α)-3-Brom-5-<(4-methylphenylsulfonyl)amino>-7-oxabicyclo<4.1.0>heptan-2,4-diol

: 112297-35-5
DL-(1α,2β,3α,4α,5β,6α)-3-Brom-5-<(4-methylphenylsulfonyl)amino>-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

: 112297-36-6
DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

Guidance literature:: With dmap; In pyridine; at 5 ℃; for 12h;

Reference yield:

: 112346-61-9
DL-(1α,2α,3β,6β)-2-Brom-6-<(4-methylphenylsulfonyl)amino>-4-cyclohexen-1,3-diol

: 112297-36-6
DL-(1α,2β,3α,4α,5β,6α)-5--3-brom-7-oxabicyclo<4.1.0>heptan-2,4-diol-diacetat

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / m-chloroperbenzoic acid, K₂HPO₄ / tetrahydrofuran; CH₂Cl₂ / 6 h / Heating

2: 10 percent / 4-(dimethylamino)pyridine / pyridine / 12 h / 5 °C

With dmap; dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; dichloromethane;