(6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

Base Information

Chemical Name:(6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester
CAS No.:35390-68-2
Molecular Formula:C₂₁H₂₁N₅O₈S
Molecular Weight:503.492
Hs Code.:

(6<i>R</i>)-3-acetoxymethyl-7<i>t</i>-((<i>R</i>)-2-azido-2-phenyl-acetylamino)-8-oxo-(6<i>r</i><i>H</i>)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

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Chemical Property of (6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

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Technology Process of (6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

There total 4 articles about (6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58-71-9
sodium cephalothin

: 35390-68-2
(6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: (i), (ii) MCPBA

2: PCl₃ / Heating

3: (i) PCl₅, (ii) nPrOH

4: py

With pyridine; phosphorus trichloride;
DOI:10.7164/antibiotics.24.767

Reference yield:

: 35390-65-9
(6R)-3-acetoxymethyl-5ξ,8-dioxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5λ⁴-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

: 35390-68-2
(6R)-3-acetoxymethyl-7t-((R)-2-azido-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid acetoxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₃ / Heating

2: (i) PCl₅, (ii) nPrOH

3: py

With pyridine; phosphorus trichloride;
DOI:10.7164/antibiotics.24.767