1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol

Base Information

• Chemical Name: 1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol
• CAS No.: 50564-94-8
• Molecular Formula: C₁₄H₂₀O₃
• Molecular Weight: 236.311
• Mol file: 50564-94-8.mol

Synonyms:

Chemical Property of 1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol

There total 1 articles about 1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol (50564-94-8)

Guidance literature:

entspr. Cyclohexanon, Lithiumacetylid;

DOI:10.1246/bcsj.46.2565

Reference yield:

1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol (50564-94-8) → 2-ethynyl-3,4,5,6-tetrahydrobenzaldehyde (21403-36-1)

Guidance literature:

With sulfuric acid; In tetrahydrofuran;

DOI:10.1246/bcsj.46.2565

Reference yield:

1-Ethinyl-2-tetrahydropyranoxymethylencyclohexanol (50564-94-8) → Bis(2-formyl-1-cyclohexenyl)-1,3-butadiin (50564-97-1)

Guidance literature:

Multistep reaction; (i) Cu(OAc)2*H₂O, Py, (ii) aq. H₂SO₄, THF;

DOI:10.1246/bcsj.46.2565

Downstream raw materials:

2-ethynyl-3,4,5,6-tetrahydrobenzaldehyde

Bis(2-formyl-1-cyclohexenyl)-1,3-butadiin