2-hydroxyacetophenone morpholine-3-thiosemicarbazone

Base Information

Chemical Name:2-hydroxyacetophenone morpholine-3-thiosemicarbazone
CAS No.:139326-54-8
Molecular Formula:C₁₃H₁₇N₃O₂S
Molecular Weight:279.363
Hs Code.:

Synonyms:

Suppliers and Price of 2-hydroxyacetophenone morpholine-3-thiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-hydroxyacetophenone morpholine-3-thiosemicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-hydroxyacetophenone morpholine-3-thiosemicarbazone

There total 1 articles about 2-hydroxyacetophenone morpholine-3-thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6499-15-6
4-morpholinothiosemicarbazide

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 139326-54-8
2-hydroxyacetophenone morpholine-3-thiosemicarbazone

Guidance literature:: In ethanol; for 12h; Heating;

Reference yield: 70.0%

: 139326-54-8
2-hydroxyacetophenone morpholine-3-thiosemicarbazone

: 62-38-4
phenylmercury(II)acetate

: [PhHg(2-hydroxyacetopenone morpholine N-thiohydrazone^(1-))]

Guidance literature:: In ethanol; EtOH soln. of PhHgOAc added to the EtOH soln. of hydrazone deriv.; refluxed for 30 min; filtered while hot; crystd. by cooling; recrystd. from EtOH; elem. anal.;
DOI:10.1016/j.poly.2009.01.002

Reference yield:

: 12440-03-8,772292-34-9,121437-28-3,22534-68-5
vanadium(IV) oxide sulfate hydrate

: 139326-54-8
2-hydroxyacetophenone morpholine-3-thiosemicarbazone

: VO⁽²⁺⁾*O(CH₂)4NC(S)N₂C(CH₃)(C₆H₄O)^(2-)*2H₂O=VO(O(CH₂)4NC(S)N₂C(CH₃)(C₆H₄O))*2H₂O

Guidance literature:: In methanol; water; treating aq. methanolic solns. of V-salt and org. ligand, refluxing on steam-bath for 0.5 h; complex sepn. by concn. or pH raising (aq. soln. of sodium acetate); complex filtration, washing (aq. methanol) and drying (CaCl2); elem. anal.;