Pleurotin

Base Information

Chemical Name:Pleurotin
CAS No.:113033-32-2
Molecular Formula:C₂₁H₂₂O₅
Molecular Weight:354.403
Hs Code.:

Synonyms:

Suppliers and Price of Pleurotin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pleurotin

Chemical Property:

Purity/Quality:

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Technology Process of Pleurotin

There total 6 articles about Pleurotin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 112946-29-9
Dihydropleurotin acid

: 1404-23-5,113033-32-2
Pleurotin

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1021/ja00201a035

Reference yield:

: 112946-40-4
rel-(3S,4S,4aS,7R,7aR,12bS,12cR)-2,3,4,4a,5,6,7,7a,8,12b-Decahydro-7-hydroxy-9,12-dimethoxy-3-methyl-12cH-4,12c-ethanoanthra<9,1-bc>oxepin

: 1404-23-5,113033-32-2
Pleurotin

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) (COCl₂)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, 50 min, 2.) 60 min

2: 1.) t-BuOK / 1.) DME, 8 min

3: 93 percent / i-Bu₂AlH / toluene / 1.65 h

4: 62 percent / Ag₂O, aq. NaOH / 23 h / 80 - 84 °C

5: 89 percent / ceric ammonium nitrate / acetonitrile; diethyl ether; H₂O / 0.5 h

6: 32 percent / active MnO₂ / CH₂Cl₂ / 48 h / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; ammonium cerium(IV) nitrate; (COCl₂)2; potassium tert-butylate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; silver(l) oxide; In diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja00201a035

Reference yield:

: 112946-41-5
rel-(3S,4S,4aS,7aR,12bS,12cR)-2,3,4,4a,5,6,7,7a,8,12b-Decahydro-9,12-dimethoxy-3-methyl-7-oxo-12cH-4,12c-ethanoanthra<9,1-bc>oxepin

: 1404-23-5,113033-32-2
Pleurotin

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) t-BuOK / 1.) DME, 8 min

2: 93 percent / i-Bu₂AlH / toluene / 1.65 h

3: 62 percent / Ag₂O, aq. NaOH / 23 h / 80 - 84 °C

4: 89 percent / ceric ammonium nitrate / acetonitrile; diethyl ether; H₂O / 0.5 h

5: 32 percent / active MnO₂ / CH₂Cl₂ / 48 h / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; ammonium cerium(IV) nitrate; potassium tert-butylate; diisobutylaluminium hydride; silver(l) oxide; In diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja00201a035