(S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester

Base Information

• Chemical Name: (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester
• CAS No.: 34029-18-0
• Molecular Formula: C₃₉H₄₂N₄O₈
• Molecular Weight: 694.784

Synonyms:

Chemical Property of (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester

There total 4 articles about (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxycarbonyl-N-(2-t.butoxycarbonylaminoethyl)glycine (34046-07-6) → (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester (34029-18-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N, DCC / dimethylformamide

2: (i) CF₃CO₂H, aq. HCl, Et₃N, DMF, (ii) /BRN= 2222826/, ClCO₂iBu, N-methylmorpholine

With triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1039/j39710003393

Reference yield:

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride (7524-50-7) → (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester (34029-18-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N, DCC / dimethylformamide

2: (i) CF₃CO₂H, aq. HCl, Et₃N, DMF, (ii) /BRN= 2222826/, ClCO₂iBu, N-methylmorpholine

With triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1039/j39710003393

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → (S)-2-(2-{Benzyloxycarbonyl-[2-((S)-2-benzyloxycarbonylamino-3-phenyl-propionylamino)-ethyl]-amino}-acetylamino)-3-phenyl-propionic acid methyl ester (34029-18-0)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) aq. NaOH, EtOH, (ii) /BRN= 509751/

2: Et₃N, DCC / dimethylformamide

3: (i) CF₃CO₂H, aq. HCl, Et₃N, DMF, (ii) /BRN= 2222826/, ClCO₂iBu, N-methylmorpholine

With triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1039/j39710003393

upstream raw materials:

N-Cbz-L-Phe

Boc-(z)-AEG-L-phenylalaninmethylester

N-benzyloxycarbonyl-N-(2-t.butoxycarbonylaminoethyl)glycine

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

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