methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate

Base Information

Chemical Name:methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate
CAS No.:117957-85-4
Molecular Formula:C₂₈H₃₈O₄
Molecular Weight:438.607
Hs Code.:

Synonyms:

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Chemical Property of methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate

Chemical Property:

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Technology Process of methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate

There total 10 articles about methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121525-78-8
3(R),6(R)-dibenzoyloxy-4(R),5(R)-dihydroxy-4,5-O-methylethylidene-1,8-octanedial

: 117957-85-4
methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate

Guidance literature:: Multi-step reaction with 6 steps

1: 1) BuLi / 1) THF, -78 deg C, 1h, 2) -78 deg to r.t., 2h

2: 100 percent / CF₃COOH / H₂O / 0.5 h / -5 °C

3: Pb(OAc)4 / CH₂Cl₂ / 0.5 h / -10 °C

4: NEt₃ / benzene / 24 h / 25 °C

5: 1) SiH₃-NLi-SiH₃, HMPA / 1) THF, 0 deg C, 2) -78 deg C

6: diethyl ether

With lead(IV) acetate; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; lithium disilylamide; triethylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; water; benzene;

Reference yield:

: 121525-79-9
2(R)-benzoyloxy-4(Z),7(Z)-tridecadienal

: 117957-85-4
methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃ / benzene / 24 h / 25 °C

2: 1) SiH₃-NLi-SiH₃, HMPA / 1) THF, 0 deg C, 2) -78 deg C

3: diethyl ether

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium disilylamide; triethylamine; In diethyl ether; benzene;

Reference yield:

: 121525-77-7
4(R),7(R)-dibenzoyloxy-5(R),6(R)-O-methylethylidene-1,9-decadiene-5,6 diol

: 117957-85-4
methyl 9(R)-benzoyloxy-5(Z),7(E),11(Z),14(Z)-eicosatetraenoate

Guidance literature:: Multi-step reaction with 7 steps

1: 1) O₃, 2) PPh₃ / 1) CH₂Cl₂, -78 deg C, 2) -78 deg C to r.t., 24h

2: 1) BuLi / 1) THF, -78 deg C, 1h, 2) -78 deg to r.t., 2h

3: 100 percent / CF₃COOH / H₂O / 0.5 h / -5 °C

4: Pb(OAc)4 / CH₂Cl₂ / 0.5 h / -10 °C

5: NEt₃ / benzene / 24 h / 25 °C

6: 1) SiH₃-NLi-SiH₃, HMPA / 1) THF, 0 deg C, 2) -78 deg C

7: diethyl ether

With lead(IV) acetate; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; lithium disilylamide; ozone; triethylamine; triphenylphosphine; trifluoroacetic acid; In diethyl ether; dichloromethane; water; benzene;