3,4,16,17-Tetraphenylheptacyclo<17.7.1.1^6,10.0^2,5.0^14,28.0^15,18.0^23,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen

Base Information

• Chemical Name: 3,4,16,17-Tetraphenylheptacyclo<17.7.1.1^6,10.0^2,5.0^14,28.0^15,18.0^23,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen
• CAS No.: 32659-60-2
• Molecular Formula: C₅₂H₄₀
• Molecular Weight: 664.89
• Mol file: 32659-60-2.mol

Synonyms:

Chemical Property of 3,4,16,17-Tetraphenylheptacyclo<17.7.1.1^6,10.0^2,5.0^14,28.0^15,18.0^23,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4,16,17-Tetraphenylheptacyclo<17.7.1.1^6,10.0^2,5.0^14,28.0^15,18.0^23,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen

There total 1 articles about 3,4,16,17-Tetraphenylheptacyclo<17.7.1.1^6,10.0^2,5.0^14,28.0^15,18.0^23,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

(E,E)-1,8-bis(2-phenylethenyl)naphthalene (30750-56-2) → 3,4,16,17-Tetraphenylheptacyclo<17.7.1.16,10.02,5.014,28.015,18.023,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen (32659-60-2)

Guidance literature:

In benzene; Ambient temperature; Irradiation;

Reference yield:

3,4,16,17-Tetraphenylheptacyclo<17.7.1.16,10.02,5.014,28.015,18.023,27>-octacosa-1(26),6,8,10(28),11,13,19,21,23(27),24-decaen (32659-60-2) → Zethren (214-63-1)

Guidance literature:

Multistep reaction; (i) (pyrolysis), (ii) (heating);

DOI:10.1021/ja00732a029

upstream raw materials:

(E,E)-1,8-bis(2-phenylethenyl)naphthalene

Downstream raw materials:

Zethren

Refernces

• 1、 Meier, Herbert,Prass, Ellen,Zertani, Rudolf,Eckes, Heinz-Ludwig. "Naphthalenophanes by Twofold Photocyclodimerization Reactions of Distyrylnaphthalenes". . p. 2139 - 2147. Retrieved 2007/10/02.