Technology Process of C33H38Cl2N4O8S3
There total 7 articles about C33H38Cl2N4O8S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 86 percent / Et3N / CH2Cl2
2.1: 80 percent / (COCl)2 / benzene / Heating
3.1: LiHMDS / tetrahydrofuran / -78 °C
3.2: 45 percent / TFA / benzene / Heating
4.1: Lawesson's reagent / toluene / 80 °C
5.1: ethanol
6.1: TBAF / tetrahydrofuran
7.1: methanol; CH2Cl2
With
Lawessons reagent; oxalyl dichloride; tetrabutyl ammonium fluoride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; benzene;
DOI:10.1016/S0960-894X(01)00060-9
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 80 percent / (COCl)2 / benzene / Heating
2.1: LiHMDS / tetrahydrofuran / -78 °C
2.2: 45 percent / TFA / benzene / Heating
3.1: Lawesson's reagent / toluene / 80 °C
4.1: ethanol
5.1: TBAF / tetrahydrofuran
6.1: methanol; CH2Cl2
With
Lawessons reagent; oxalyl dichloride; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; benzene;
DOI:10.1016/S0960-894X(01)00060-9
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: LiHMDS / tetrahydrofuran / -78 °C
1.2: 45 percent / TFA / benzene / Heating
2.1: Lawesson's reagent / toluene / 80 °C
3.1: ethanol
4.1: TBAF / tetrahydrofuran
5.1: methanol; CH2Cl2
With
Lawessons reagent; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; toluene;
DOI:10.1016/S0960-894X(01)00060-9
