ethyl 4-nitrophenylphosphonochloridate

Base Information

Chemical Name:ethyl 4-nitrophenylphosphonochloridate
CAS No.:166522-34-5
Molecular Formula:C₈H₉ClNO₄P
Molecular Weight:249.591
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-nitrophenylphosphonochloridate

Chemical Property:

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Technology Process of ethyl 4-nitrophenylphosphonochloridate

There total 2 articles about ethyl 4-nitrophenylphosphonochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1754-42-3
para-nitro-phenylphosphonate diethylique

: 166522-34-5
ethyl 4-nitrophenylphosphonochloridate

Guidance literature:: With phosphorus pentachloride; In benzene; r.t, 24 h, then reflux for 1 h;
DOI:10.1002/ardp.19933260403

Reference yield:

: 166522-34-5
ethyl 4-nitrophenylphosphonochloridate

Guidance literature:

Reference yield:

: 166522-34-5
ethyl 4-nitrophenylphosphonochloridate

: 4-Aminophenylphosphonsaeureethylester-(4,6-dimethylpyrimidin-2-yl)-amid

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 1 h / Heating

2: 92 percent / hydrogen / Raney-nickel / tetrahydrofuran / 760 Torr

With hydrogen; triethylamine; nickel; In tetrahydrofuran;
DOI:10.1002/ardp.19933260403