tris(dicyclohexylacetamide)dichlorodiisothiocyanatothorium(IV)

Base Information

Chemical Name:tris(dicyclohexylacetamide)dichlorodiisothiocyanatothorium(IV)
CAS No.:144071-76-1
Molecular Formula:C₄₄H₇₅Cl₂N₅O₃S₂Th
Molecular Weight:1089.19
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(dicyclohexylacetamide)dichlorodiisothiocyanatothorium(IV)

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Technology Process of tris(dicyclohexylacetamide)dichlorodiisothiocyanatothorium(IV)

There total 1 articles about tris(dicyclohexylacetamide)dichlorodiisothiocyanatothorium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 89140-66-9
tris(dicyclohexylacetamide)tetrachlorothorium(IV)

: 1563-91-3
N,N-dicyclohexylacetamide

: 144071-76-1,93267-73-3
tris(dicyclohexylacetamide)dichlorodiisothiocyanatothorium(IV)

Guidance literature:: With potassium thioacyanate; In tetrahydrofuran; addn. of 0.29 mmol acetamide and 0.58 mmol KNCS to a stirred soln. of 0.29 mmol tetrachloro compound in 10 ml THF, stirring for 72 h at 25°C; performed under N2;; evapn.; dissolving in CH2Cl2 and addn. of n-pentane; crystallization within a few hours; washing with n-pentane and drying in vacuum (5 h); elem. anal.;;
DOI:10.1016/0022-5088(84)90390-4